|本期目录/Table of Contents|

[1]孙晓英,肖安山,魏新明,等.加油站埋地罐区土壤中油气含量检测方法研究[J].中国安全生产科学技术,2014,10(1):64-67.[doi:10.11731/j.issn.1673-193x.2014.01.010]
　SUN Xiao ying,XIAO An shan,WEI Xin ming,et al.Research on detection methon of TPH (Total Petroleum Hydrocarbons) in soil of UST (Underground Storage Tank) in gas station[J].JOURNAL OF SAFETY SCIENCE AND TECHNOLOGY,2014,10(1):64-67.[doi:10.11731/j.issn.1673-193x.2014.01.010]
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加油站埋地罐区土壤中油气含量检测方法研究
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《中国安全生产科学技术》[ISSN:1673-193X/CN:11-5335/TB]

卷:
10
期数:
2014年1期
页码:
64-67
栏目:
学术论著
出版日期:
2014-01-28

文章信息/Info

Title:
Research on detection methon of TPH (Total Petroleum Hydrocarbons) in soil of UST (Underground Storage Tank) in gas station
作者:
孙晓英1; 2; 肖安山1; 2; 魏新明1; 2; 胡绪尧1; 2; 马明1; 2
(1 中国石化青岛安全工程研究院，山东青岛266071； 2 化学品安全控制国家重点实验室，山东青岛266071)
Author(s):
SUN Xiaoying1; 2; XIAO Anshan1; 2;  WEI Xinming1; 2;  HU Xuyao1; 2;  MA Ming1; 2
(1SINOPEC Safety Engineering Institute，Qingdao Shandong 266071, China; 2 State Key Laboratory of Safety and Control for Chemicals，Qingdao Shandong 266071 ,China)
关键词:
探地雷达; 土壤; 油气含量; 气相色谱法
Keywords:
ground penetrating radar;  soil;  total petroleum hydrocarbons;  chromatography
分类号:
X937
DOI:
10.11731/j.issn.1673-193x.2014.01.010
文献标志码:
A
摘要:
以某加油站埋地罐区为例，针对探地雷达法验证实验的需要，建立了以手动钻孔取样，以有机溶剂二氯甲烷进行萃取，采用气相色谱法进行定量的土壤中油气含量分析方法，并对方法的线性、检出限、加标回收率等进行了研究。气相色谱分析结果表明用二氯甲烷替代四氯化碳作为土壤中油气含量测定的萃取剂，萃取结果良好；探地雷达法测得的1号罐和3号罐泄漏区域土壤中油气含量高达8564mg/kg和7723mg/kg，证明探底雷达法可以迅速检测到埋地罐区泄漏区域。
Abstract:
In order to validate the ground penetrating radar (GPR) method, the gas chromatography test was done. Based on the rule of similarity, the organic solvent methylene dichloride was used for extracting the sample of soil around underground storage tank in the gas station. The contents of TPH(Total Petroleum Hydrocarbons) in soil was detected by gas chromatography, and the parameters about limit of detection and recovery rate were checked. The result showed that the extraction results was better when carbon tetrachloride was replaced by methylene chloride as extracting agent for the determination of oil and gas content in the soil. The concert of TPH in soil around tank 1 and tank 3 were up to 8564mg/kg and 7723mg/kg respectively, and GPR method could quickly detect the leaked area of underground storage tank.

参考文献/References:

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备注/Memo

备注/Memo:
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更新日期/Last Update: 2014-01-30