|本期目录/Table of Contents|

[1]姬文苏,曹宏安,赵东华,等.湿法粉碎制备纳米RDX安全性分析与性能表征[J].中国安全生产科学技术,2016,12(3):26-29.[doi:10.11731/j.issn.1673-193x.2016.03.005]
 JI Wensu,CAO Hongan,ZHAO Donghua,et al.Safety analysis and characterization on nanometer RDX produced by wet grinding[J].JOURNAL OF SAFETY SCIENCE AND TECHNOLOGY,2016,12(3):26-29.[doi:10.11731/j.issn.1673-193x.2016.03.005]
点击复制

湿法粉碎制备纳米RDX安全性分析与性能表征
分享到:

《中国安全生产科学技术》[ISSN:1673-193X/CN:11-5335/TB]

卷:
12
期数:
2016年3期
页码:
26-29
栏目:
学术论著
出版日期:
2016-03-30

文章信息/Info

Title:
Safety analysis and characterization on nanometer RDX produced by wet grinding
文章编号:
1673-193X(2016)-03-0026-04
作者:
姬文苏曹宏安赵东华谷智国李惠明
(武汉军械士官学校,湖北 武汉 430075)
Author(s):
JI Wensu CAO Hongan ZHAO Donghua GU Zhiguo LI Huiming
(Wuhan N.C.O. Academy of P.L.A.,Wuhan Hubei 430075, China)
关键词:
材料科学纳米RDX粉碎感度安全
Keywords:
material sciencenanometer RDX grinding sensitivity safety
分类号:
X959
DOI:
10.11731/j.issn.1673-193x.2016.03.005
文献标志码:
A
摘要:
从热传导理论分析入手,以回收的RDX为原料,选择易获取的水为导热介质,湿法粉碎制备了纳米级RDX样品。利用纳米激光粒度仪、场发射扫描电镜和卡斯特型落锤仪对样品粒径大小、外观特征、感度大小进行了观察和测试。实验结果表明,湿法制备的纳米级RDX感度明显降低,安全性提高。由于本方法成本低廉,使得大规模回收的RDX再次利用成为可能,解决了RDX不方便储存运输使用等难题,扩大了其使用范围。
Abstract:
Starting from the theoretical analysis of heat conduction, taking the recovered RDX as raw material and selecting the water which is easy to be obtained as heat conduction media, the sample of nanometer RDX was produced by wet grinding. The particle size distribution, appearance characteristics and sensitivity of sample were observed and tested by using the nanometer laser particle size analyzer, field emission scanning electron microscope and Custer type drop hammer machine. The results showed that for the nanometer RDX produced by wet grinding, the sensitivity was reduced significantly and the safety was improved. The low cost of this method make it possible to reuse the recovered RDX on a large scale, the difficult problems of RDX being inconvenient to store, transport and use were solved, which enlarges its application range.

参考文献/References:

[1]姬文苏,丁玉奎,李金明,等.超临界CO2流体分离梯黑炸药的响应曲面法优化研究[J].火工品,2011(4):36-39. JI Wensu, DING Yukui, LI Jinming,et al. Optimization on supercritical carbon dioxide separating TNT and RDX explosive with response surface methodology[J].Initiators&Pyrotechnics,2011(4):36-39.
[2]姬文苏,丁玉奎,李金明,等.某混合炸药提取铝工艺与动力学研究[J].化学工业与工程,2011,28(4):16-21. JI Wensu, DING Yukui, LI Jinming,et al. Technology and kinetics of leaching Al from mixed explosive[J]. Chemical Industry and Engineering,2011,28(4):16-21.
[3]丁玉奎,吴翼,刘国庆,等.熔融法分离废弃梯黑铝炸药中的TNT[J].含能材料,2014,22(4):548-553.DING Yukui, WU Yi, LIU Guoqing,et al. Separation of TNT from discarded or obsolete TNT/RDX/Al explosives by melting method[J]. Chinese Journal of Energetic Materials,2014,22(4):548-553.
[4]吴翼,丁玉奎,刘国庆,等.溶剂萃取法回收废旧梯黑铝炸药中的RDX和铝粉[J].火炸药学报,2014,37(6):35-39. WU Yi , DING Yukui , LIU Guoqing,et al. Recovery of RDX and Al powder in discarded or obsolete TNT/RDX/Al explosive by solvent extraction[J]. Chinese Journal of Explosives & Propellants,2014,37(6):35-39.
[5]张晋元.壳体厚度对传爆药慢速烤燃响应的研究[J].中国安全生产科学技术,2011,7(3):61-64. ZHANG Jinyuan. Study of influence of shell thickness on the response of booster explosive in slow cook-off test[J]. Journal of Safety Science and Technology,2011,7(3):61-64.
[6]陈厚和,孟庆刚,曹虎,等.纳米RDX粉体的制备与撞击感度[J].爆炸与冲击,2004,24(4):382-384. CHEN Houhe,MENG Qinggang,CAO Hu,et al. Preparation and impact sensitivity of nanometer explosive powder of RDX[J]. Explosion and Shock Waves,2004,24(4):382-384.
[7]宋小兰,李凤生,张景林,等.纳米RDX的制备及其机械感度和热分解特性[J].火炸药学报,2008,31(6):1-4. SONG Xiaolan, LI Fengsheng , ZHANG Jinglin,et al. Preparation, mechanical sensitivity and thermal decomposition characteristics of RDX nanoparticles[J]. Chinese Journal of Explosives & Propellants,2008,31(6):1-4.
[8]Radacsi N,Stankiewicz A I,Creyghton Y L M,et al.Electrospray crystallization for high-quality submicron-sized crystals[J].Chem Eng Techn,2011,34(4):624.
[9]Stepano V,Krasnoperov L N,Elkina I B,et al.Production of nanocrystalline RDX by rapid expansion of supercritical solutions[J].Propel Explos Pyrotechn,2005,30(3):178.
[10]Klapoetke,tm. Insensitive High-performance Replacements for RDX in Explosive and Propellant Formulations[R].ADA466070/XAB,2007.
[11]王志军,尹建平.弹药学[M].北京:北京理工大学出版社,2005.
[12]GJB 772A-97.炸药实验方法[S].北京:国防科工委军标发行部,1997.
[13]杜仕国,杨建武,高俊国.火炸药学[M].石家庄:军械工程学院出版社,1999.

相似文献/References:

备注/Memo

备注/Memo:
军队部级科研项目(【2014】80);武汉军械士官学校青年创新基金项目
更新日期/Last Update: 2016-04-15