|本期目录/Table of Contents|

[1]周彪,方尘逸,孙绪坤,等.浸渍法提高石墨安全性能的研究*[J].中国安全生产科学技术,2021,17(8):156-161.[doi:10.11731/j.issn.1673-193x.2021.08.024]
 ZHOU Biao,FANG Chenyi,SUN Xukun,et al.Research on improving safety performance of graphite by dipping method[J].JOURNAL OF SAFETY SCIENCE AND TECHNOLOGY,2021,17(8):156-161.[doi:10.11731/j.issn.1673-193x.2021.08.024]
点击复制

浸渍法提高石墨安全性能的研究*
分享到:

《中国安全生产科学技术》[ISSN:1673-193X/CN:11-5335/TB]

卷:
17
期数:
2021年8期
页码:
156-161
栏目:
职业安全卫生管理与技术
出版日期:
2021-08-31

文章信息/Info

Title:
Research on improving safety performance of graphite by dipping method
文章编号:
1673-193X(2021)-08-0156-06
作者:
周彪方尘逸孙绪坤李玥蓉柯巍韩腾奔
(1.中国矿业大学(北京) 应急管理与安全工程学院,北京 100083;
2.武汉船用电力推进装置研究所,湖北 武汉 430000)
Author(s):
ZHOU Biao FANG Chenyi SUN Xukun LI Yuerong KE Wei HAN Tengben
(1.College of Emergency Management and Safety Engineering,China University of Mining and Technology (Beijing),Beijing 100083,China;
2.Wuhan Marine Electric Propulsion Research Institute,Wuhan Hubei 430000,China)
关键词:
石墨电极浸渍生产安全优化配比抗氧化
Keywords:
graphite electrode dipping production safety optimized ratio anti-oxidation
分类号:
X937
DOI:
10.11731/j.issn.1673-193x.2021.08.024
文献标志码:
A
摘要:
为提高石墨电极的安全性能,采用浸渍法讨论不同活性组分负载的石墨样品在750 ℃环境下的抗氧化性能及影响机制。通过一系列单一活性组分筛选实验和复合活性组分筛选实验讨论活性组分对单位面积质量损失的影响,验证组分优选的可靠性;通过浓度变量实验,得到复合组分浸渍液的优化配比。根据石墨的微观结构和元素组分变化,提出活性组分抗氧化作用机理。结果表明:活性组分与石墨在高温作用下形成的络合物层能够有效延长石墨电极的使用寿命,提高生产安全水平。
Abstract:
In order to improve the safety performance of graphite electrodes,the dipping method was used to discuss the anti-oxidation performance and influence mechanism of graphite samples with different active components load in 750 ℃ environment.The influence of the active components on the mass loss per unit area was discussed through a series of single active component and composite active components screening experiments,and the reliability of component optimization was verified.Through the concentration variable experiments,the optimal ratio of the composite component dipping solution was obtained.According to the microstructure and element composition variation of graphite,the anti-oxidation mechanism of the active component was proposed.The results showed that the complex layer formed by the active components and graphite under the effect of high temperature could prolong the service life of the graphite electrode,and improve the level of production safety.

参考文献/References:

[1]张波.矿渣微粉-糊精灰浆复合胶凝材料的试验研究 [J].硅酸盐通报,2020,39(4):1208-1213. ZHANG Bo.Experimental study on slag powder-dextrin mortar composite cementitious materials [J].Bulletin of the Chinese Ceramic Society,2020,39(4):1208-1213.
[2]邓亚利,仉小猛,魏连启,等.两步溶液浸渍法提高石墨材料的高温抗氧化性能 [J].过程工程学报,2012,12(1):160-165. DENG Yali,ZHANG Xiaomeng,WEI Lianqi,et al.Improvement inanti-oxidation of two-step dipping graphite with different solutions [J].The Chinese Journal of Process Engineering,2012,12(1):160-165.
[3]王振廷,朱士奎,冯帆.石墨电极表面氩弧熔覆原位合成ZrB2-SiC/Si抗氧化涂层 [J].焊接学报,2015,36(8):55-58,116. WANG Zhenting,ZHU Shikui,FENG Fan.Research of in-suit synthesis of ZrB2-SiC/Si high temperature oxidation esistant coating on graphite by argon arc cladding [J].Transactions of the China Welding Institution,2015,36(8):55-58,116.
[4]朱宗亮.高温抗氧化柔性石墨的制备及性能研究 [D].上海:华东理工大学,2016.
[5]饶娟,张盼,何帅,等.天然石墨利用现状及石墨制品综述 [J].中国科学:技术科学,2017,47(1):13-31. RAO Juan,ZHANG Pan,HE Shuai,et al.A review on the utilization of natural graphite and graphite-based materials [J].Scientia Sinica(Technologica),2017,47(1):13-31.
[6]CHO Y,YUN R.A raw water source heat pump air-conditioning system [J].Energy & Buildings,2011,43(11):3068-3073.
[7]KLEIN S,HOUBEN L,CARIUS R,et al.Structural properties of microcrystalline SiC deposited at low substrate temperatures by HWCVD [J].Journal of Non-Crystalline Solids,2006,352(9-20):1376-1379.
[8]刘琛.SiOC基陶瓷改性碳纤维骨架复合材料及其抗氧化涂层研究 [D].哈尔滨:哈尔滨工业大学,2015.
[9]姜岩,冯东,茹红强,等.石墨表面Si-SiC-ZrB2抗氧化复合涂层的制备及性能表征 [J].耐火材料,2018,52(4):241-245. JIANG Yan,FENG Dong,RU Hongqiang,et al.Preparation and property characterization of Si-SiC-ZrB2 oxidation resistant compositecoating on graphite surface [J].Refractories,2018,52(4):241-245.
[10]谢苏江,朱宗亮.高温抗氧化柔性石墨密封材料的制备和性能研究 [J].流体机械,2017,45(2):12-16,70. XIE Sujiang,ZHU Zongliang.The preparation and performance research of high temperature oxidation resistance of graphite [J].Fluid Machinery,2017,45(2):12-16,70.
[11]朱宗亮,谢苏江,李红振.浸渍法提高柔性石墨抗氧化性能的研究 [J].非金属矿,2016,39(1):58-60,64. ZHU Zongliang,XIE Sujiang,LI Hongzhen.Study onoxidation resistance of flexible graphite by impregnation [J].Non-Metallic Mines,2016,39(1):58-60,64.
[12]LIN Y,LIU T,WANG J,et al.Fabrication and oxidation resistance behavior of phosphate/borate impregnation for graphite [J].Surface & Coatings Technology,2020,389:125632.
[13]王鹏.石墨表面耐烧蚀抗氧化复合涂层制备及性能研究 [D].哈尔滨:哈尔滨工业大学,2016.
[14]孙宏友.基于正交试验法的透水混凝土配合比设计和试验研究 [D].成都:西南交通大学,2016.
[15]张东,李秀强.石墨氧化过程中官能团及结构的变化 [J].同济大学学报(自然科学版),2014,42(9):1372-1376. ZHANG Dong,LI Xiuqiang.Changes of groups and structure on oxidation process of graphite [J].Journal of Tongji University(Natural Science),2014,42(9):1372-1376.
[16]王凌,许斌.石墨材料的抗氧化 [J].炭素科技,1999,9(4):36-44. WANG Ling,XU Bin.Anti-oxidation ofgraphite materials [J].Carbon Science and Technology,1999,9(4):36-44.

相似文献/References:

[1]徐志胜,赵雯筠,颜龙,等.羟基化氮化硼与磷酸二氢铵在致密化木材中的阻燃作用*[J].中国安全生产科学技术,2023,19(6):151.[doi:10.11731/j.issn.1673-193x.2023.06.021]
 XU Zhisheng,ZHAO Wenjun,YAN Long,et al.Flame-retardant function of hydroxylated boron nitride and ammonium dihydrogen phosphate on densified wood[J].JOURNAL OF SAFETY SCIENCE AND TECHNOLOGY,2023,19(8):151.[doi:10.11731/j.issn.1673-193x.2023.06.021]

备注/Memo

备注/Memo:
收稿日期: 2021-01-07
* 基金项目: 中央高校基本科研业务费项目(2020XJAQ03);国家自然科学基金项目(51904311)
作者简介: 周彪,博士,讲师,主要研究方向为职业健康与工业灾害防治。
更新日期/Last Update: 2021-09-08